Copper oxides are important for superconductivity applications but are difficult to understand due to complex charge, spin, and orbital interactions. Now, studies at the ALS have found such a system in which observations of effective electron mass are at odds with state-of-the-art electronic-structure calculations. Read more »
Science Briefs
Formation of a Photovoltaic Material from Precursor to Crystal
Lead halide perovskites have emerged as high-performance photovoltaic materials, demonstrating remarkably rapid improvements in efficiency. In situ printing and time-resolved x-ray characterization have provided new insights into the relationship between device efficiency, perovskite crystallinity, and film morphology. Read more »
Hybrid LED Phosphors Combine Performance and Durability
Light-emitting diodes (LEDs) last a long time and are very energy efficient. However, white LEDs currently rely on phosphor materials doped with rare-earth elements (REEs) that are increasingly costly and in short supply. A new class of hybrid phosphor materials shows promise as REE-free alternatives. Read more »
The Ancient Roman Secret to Concrete Resilience in Seawater
Researchers used x-ray microdiffraction to trace the complex sequences of crystal growth in concrete from ancient Roman pier and breakwater sites. The results indicate that minerals continue to form over millennia as seawater percolates through, reinforcing the cementing matrix in a kind of regenerative process. Read more »
Fine-Tuning Oxygen Vacancies with Coherent Strain
Researchers have demonstrated a novel way to systematically strain-engineer oxygen vacancies in complex transition-metal oxide thin films. The work advances our ability to tailor such defects, small changes in which can lead to dramatic changes in material properties such as conductivity and magnetism. Read more »
Protein Complex Shows Promise for Berkelium Separation
Scientists found that the element berkelium breaks form with its heavy-element peers by taking on an extra positive charge when bound to a synthetic organic molecule. This property could help scientists develop better methods for handling and purifying nuclear materials. Read more »
A Systematic Approach to Customizing Cyclic Proteins
Proteins consisting of identical subunits arranged symmetrically around a central axis (cyclic homo-oligomers) play key roles in many biological processes. Researchers have now developed a systematic approach to their design and demonstrated its accuracy using protein crystallography and small-angle x-ray scattering. Read more »
Bacterial Symbiont Sequesters Arsenic and Barium in Sponges
Researchers used x-ray fluorescence, spectroscopy, and diffraction to study how populations of symbiotic bacteria can act as a detox organ in a host with no organs. The bacteria, members of the species Entotheonella, accumulate and mineralize large quantities of arsenic and barium in sponges. Read more »
A Closer Look at a Working Platinum/Electrolyte Interface
Ambient-pressure studies of the interface between a platinum electrode and an alkaline electrolyte revealed the molecular-level chemistry, structure, and dynamics of the platinum surface as a function of applied potential, highlighting differences between thermodynamic predictions and the actual surface composition. Read more »
A Hollow Pyramid Unlocks Principles of Protein Architecture
Researchers have designed a hollow, pyramid-shaped protein with a controllable cavity size that could be useful in the capture and release of smaller compounds. The tools and techniques developed could be useful in analyzing and optimizing designed protein assemblies and understanding their behavior in solution. Read more »
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