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Science Briefs

To Speed Discovery, Infrared Microscopy Goes “Off the Grid”

Researchers developed a highly efficient way to collect infrared microscopy data that avoids the use of slow, grid-based raster scans. The method substantially reduces image-acquisition times by autonomously increasing sampling density in regions of interest, facilitating infrared spectromicroscopy of biochemical processes in real time. Read more »

Actor in a Supporting Role: Substrate Effects on 2D Layers

ALS studies highlighted interactions that can occur between technologically intriguing 2D materials and the substrates that physically support them. The results provide important insights into the issue of non-negligible interlayer coupling and demonstrate the potential for tuning single-layer properties through substrate engineering. Read more »

Stacking the Deck for Custom-Built Hybrid Materials

Researchers fabricated an electronically coupled heterostructure from a novel semiconducting 2D polymer and a 2D transition metal dichalcogenide. Dramatic optical and electronic changes emerged as polymer thickness decreased, underscoring the potential for the discovery of emergent phenomena in studies of hybrid heterostructures. Read more »

Newly Discovered Photosynthesis Enzyme Yields Evolutionary Clues

Scientists have discovered a primitive form of rubisco, a photosynthesis enzyme that has helped shape life on Earth. Detailed information about its structure, determined using complementary techniques at the ALS, will help scientists understand how carbon-fixing organisms oxygenated the atmosphere and how modern plants evolved. Read more »

Detecting Phonon Overtones in Correlated Materials

Resonant inelastic x-ray scattering (RIXS) has recently been shown to be a promising technique for studying electron–phonon coupling in correlated materials. When a photoexcited electron interacts with phonons during decay, it shows up in the RIXS spectra as clear phonon overtones: higher-order excitations that appear as ripples in intensity. Read more »

Stress-Induced Structural Transformations in Gold Nanocrystals

Metallic nanocrystals are widely used in catalysis, electronics, photonics, and sensing applications, but our understanding of their stability under operational stresses is limited. These studies of gold nanocrystals at high pressures found that large-scale structural transformation is possible and must be considered at the nanoscale. Read more »

Understanding Electronic Structure in MXenes, One Atomic Layer at a Time

MXenes are 2D materials that can host a rich array of distinct chemical compositions that can be tuned for a broad range of applications, from energy storage to water purification. Site-specific x-ray absorption spectroscopy helped identify the unique roles of surface and subsurface transition-metal atoms in Ti-based MXenes. Read more »

Characterization of EUV Optics using Intrinsic Mask Roughness

Researchers developed an in situ computational technique for measuring aberrations in EUV optics, taking advantage of the surface roughness of photomasks used to transfer circuit patterns onto chips. The technique will prove increasingly valuable in the characterization of coherent light sources and beamline optical systems. Read more »

Missing Lysine Link Could Improve Plant-Based Nutrition

To engineer crops with higher levels of the important amino acid, lysine, researchers solved the structure of an enzyme that helps break down lysine in plants. A fuller understanding of the factors affecting lysine levels should aid in the successful development of stable high-lysine crops to combat malnutrition globally. Read more »