Using 3D x-ray microtomography, researchers measured the lithiation levels of particles in Li-ion battery electrodes during charging. At faster charging rates, lithium metal accumulated on the electrode surface and created a “shadow effect,” a region of poor lithiation in the electrode at some distance away from the lithium plating. Read more »
Science Briefs
When Timing Isn’t Everything: Spontaneous Chemical Dynamics
Researchers combined aspects of x-ray photoelectron spectroscopy (XPS) with correlation spectroscopy—a statistical method capable of detecting patterns in microscopic fluctuations across space and time. The new technique, called time-correlation XPS, allows researchers to monitor dynamics without the need for a timed trigger. Read more »
A Powerful Infrared Technique Broadens Its Horizons
Scattering-type scanning near-field optical microscopy (s-SNOM) focuses infrared light to dimensions below the diffraction limit, measuring properties with components perpendicular to the sample surface. Researchers have now devised a way to probe components parallel to the sample, where the technique has been less sensitive. Read more »
Sifting through Fragments for COVID-19 Treatments
COVID-19 vaccines are essential for preventing serious disease, but the identification of new drugs is still necessary for the treatment of patients who become sick as a result of SARS-CoV-2 infection. Here, scientists used computational docking and crystallography to screen large numbers of small molecules for potential use in drug compounds. Read more »
A Multiscale Picture of Oxygen Loss in Battery Electrodes
In lithium-ion batteries, oxygen atoms leak out of electrode particles as the lithium moves back and forth between electrodes. Now, researchers have measured this process at multiple length scales, showing how the oxygen loss changes the electrode’s structure and chemistry, gradually reducing the amount of energy it can store. Read more »
In a Hawaiian Lava Fountain, Fluid Magma Turns Brittle
Compared to the violent explosions of Mount Vesuvius or Mount St. Helens, Hawaiian volcanic eruptions are relatively calm, characterized by flowing rivers and fountains of lava. Here, researchers have discovered that even low-viscosity magma sometimes behaves more like brittle glass that shatters into fine particles. Read more »
Mineral Microstructures Shed Light on Planet-Scale Dynamics
To explore what happens to minerals under the extreme conditions in Earth’s mantle, researchers developed an x-ray technique that bridges the gap between methods that reveal bulk properties and those that focus on individual crystals. Use of the technique has shed light on the dynamics of tectonic-plate subduction in Earth’s lower mantle. Read more »
Researchers Set Sights on Another COVID-19 Target
Early in the COVID-19 pandemic, it was quickly established that the receptor binding domain (RBD) of the SARS-CoV-2 spike protein is a prime target for neutralizing antibodies. Now, scientists have found a second region of the spike protein that is targeted by dozens of antibodies, some of which exhibit ultrapotent neutralizing activity. Read more »
Scientists Uncover a Different Facet of Fuel-Cell Chemistry
Solid oxide fuel cells are a promising technology for cleanly converting chemical energy to electrical energy. To improve the efficiency of these devices, researchers studied a model electrode material in a new way—by exposing a different facet of its crystal structure to oxygen gas at operating pressures and temperatures. Read more »
New Tools Link Catalytic Activity to Nanoscale Transformations
Transitioning to a clean hydrogen economy will require cheaper, more efficient ways to split water molecules. To address bottlenecks in the water-splitting process, researchers developed a suite of advanced tools, including a liquid flow cell that enables electrochemical studies of catalysts under working conditions. Read more »
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