Machine-learning techniques have been used to integrate fine- and large-scale infrared characterizations of shale—sedimentary rocks composed of minerals and organic matter. Understanding shale chemistry at both the nano and mesoscale is relevant to energy production, climate-change mitigation, and sustainable water and land use. Read more »
ALS Work Using Spectroscopy
These techniques are used to study the energies of particles that are emitted or absorbed by samples that are exposed to the light-source beam and are commonly used to determine the characteristics of chemical bonding and electron motion.
Clarifying the Working Principle of a High-Capacity Battery Electrode
Operando x-ray absorption spectroscopy experiments revealed the electrochemical reaction mechanism of molybdenum disulfide (MoS2) electrodes in lithium-ion battery cells. The work unambiguously clarifies that the MoS2 conversion reaction is not reversible and that the Li2S formed is converted to sulfur in the first charge process. Read more »
Monovalent Manganese for High-Performance Batteries
Scientists have detected a novel chemical state of the element manganese that was first proposed about 90 years ago. The discovery enables the design of a high-performance, low-cost battery that, according to its developers, outperforms Department of Energy goals on cost and cycle life for grid-scale energy storage. Read more »
Toward Control of Spin States for Molecular Electronics
Researchers demonstrated, via x-ray absorption spectroscopy, that a molecule’s spin state can be reversibly switched at constant room temperature by magnetism. The results represent a major step toward the goal of programmable, nanoscale molecular electronics for high-speed, low-power, logic and memory applications. Read more »
Phase Diagram Leads the Way to Tailored Metamaterial Responses
Researchers discovered an innovative way to independently control two optical responses in a single-material system by utilizing the material’s phase diagram. This unique combination of material, methods, and results could lead to a paradigm shift in the design of metamaterial devices that manipulate light. Read more »
Tuning the Electronic Structure of a 2D Material
The electronic structure of a stacked 2D material was tuned by in situ electron doping, resulting in a large increase in the splitting of two valence bands. Stacked 2D materials possess an array of tunable properties that are expected to be important for future applications in electronics and optics. Read more »
Diamonds From the Deep: Study Suggests Water May Exist in Earth’s Lower Mantle
A new study suggests that water may be more common than expected at extreme depths approaching 400 miles and possibly beyond—within Earth’s lower mantle. The study explored microscopic pockets of a trapped form of crystallized water molecules in a sampling of diamonds from around the world. Read more »
Scientists Confirm Century-Old Speculation on the Chemistry of a High-Performance Battery
Scientists have discovered a novel chemical state of the element manganese. This chemical state, first proposed about 90 years ago, enables a high-performance, low-cost sodium-ion battery that could quickly and efficiently store and distribute energy produced by solar panels and wind turbines across the electrical grid. Read more »
Ingredients for Life Revealed in Meteorites
X-ray absorption spectroscopy and other techniques were used to measure the organic chemical components in a pair of meteorites that crashed to Earth in 1998. The study treads new ground in solar system history and asteroid geology, surfacing exciting possibilities for the existence of life elsewhere in Earth’s neighborhood. Read more »
The Microstructure of a Parrotfish Tooth Contributes to Its Toughness
Parrotfish chew on coral, producing hundreds of pounds of sand each year. Mapping the microstructure of parrotfish teeth, scientists found bundles of crystals interwoven like chain mail. The results provide a blueprint for creating ultra-durable materials for mechanical components that undergo repetitive contact, movement, and abrasion. Read more »
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