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ALS Work Using Spectroscopy

These techniques are used to study the energies of particles that are emitted or absorbed by samples that are exposed to the light-source beam and are commonly used to determine the characteristics of chemical bonding and electron motion.

 

Watching the Enzymes that Convert Plant Fiber into Simple Sugars

Research from Lawrence Berkeley National Laboratory, Lawrence Livermore National Laboratory, and UC Davis sheds new light on how to access the sugars locked up in plants to produce petroleum-free fuels, chemicals, and medicines. The technique used combines a novel microfluidic device and infrared spectroscopy to study how a cellulose-degrading enzyme works in real time. Read more »

Cobalt or Nickel: Which is Better for High-Energy Battery Cathodes?

High-energy Li-ion batteries can provide both high capacity and high voltage, both of which are important in electric vehicles for greater range and faster acceleration. Here, researchers untangled the contributions of nickel and cobalt in high-energy Li-rich battery cathodes, pointing the way to optimizing them via a compositional approach. Read more »

Flat Bands Signal Electrons Trapped in 3D

Researchers found flat electronic band structures—known hallmarks of electrons trapped in two dimensions—but in a material that extends this phenomenon to three dimensions. The work opens up a material framework for exploring superconductivity and other exotic states in three dimensions for advanced electronic applications. Read more »PPT-icon-35 PDF-icon-35

Tracking Platinum Movement on Fuel-Cell Electrodes

Researchers tracked the movement of the platinum nanoparticles that catalyze reactions in polymer electrolyte fuel cells (PEFCs) and correlated this movement with nanoparticle degradation. The results yielded solutions that can immediately reduce platinum waste in emission-free heavy-duty fuel-cell vehicles. Read more »PPT-icon-35 PDF-icon-35

Building a Two-Dimensional Magnet One Atom at a Time

Researchers synthesized a new two-dimensional ferromagnet and measured how its electronic and magnetic properties evolve with increasing thickness and temperature. Such atomically thin magnetic materials with tunable magnetic properties would be very useful in next-generation microelectronic and spintronic applications. Read more »

Immune Response Spurs Growth of “Soft” Kidney Stones

Matrix stones are an unusual type of soft kidney stone closely associated with the presence of bacteria from unchecked urinary tract infections. Researchers conducted a comprehensive study of surgically extracted matrix stones, work that highlights how host defense mechanisms against microbes can simultaneously encourage harmful stone formation. Read more »

HyMARC Aims to Hit Targets for Hydrogen Storage Using X-Ray Science

Understanding how materials absorb and release hydrogen is the focus of the Hydrogen Materials Advanced Research Consortium (HyMARC). At the ALS, the HyMARC Approved Program was recently renewed, underscoring the key role that soft x-ray techniques have played in addressing the challenges of hydrogen storage. Read more »

Spectroscopic investigation of a Co(0001) model catalyst during exposure to H2 and CO at near-ambient pressures

We have performed near-ambient-pressure X-ray photoelectron spectroscopy on Co(0001) model catalysts during exposure to gases relevant to Fischer–Tropsch synthesis, i.e., CO and H2, at 0.25 mbar total pressure. At this pressure, CO seems to be more efficient at keeping the Co(0001) surface metallic than H2, which is the opposite behavior as reported in the literature for other pressure ranges. Read more »

Organic Matrix Derived from Host–Microbe Interplay Contributes to Pathological Renal Biomineralization

A composite image of a rare form of kidney stone, illustrating extensive organic filamentous networks abundant with immune response-related proteins such as calprotectin (displayed in red), myeloperoxidase (in yellow), and DNA molecules (in blue). Originating from intricate host-microbe interplay, these organic networks promote the heterogeneous nucleation and precipitation of inorganic particulates. Read more »