Hydrogen is the lightest and most plentiful element on Earth and could serve as a carbon-free, virtually limitless energy source. Recently, researchers working at the ALS and the Molecular Foundry developed a promising new materials recipe based on magnesium nanocrystals and graphene for a hydrogen fuel cell with improved performance in key areas. Read more »
ALS Work Using XAS
In x-ray absorption spectroscopy (XAS), the incident x-ray energy is tuned over a range that will excite core-level electrons. Sharp increases in absorption occur at specific energies, characteristic of the absorbing element. The resulting spectra probe the elemental composition as well as the chemical and electronic structure of the material.
Missing Oxygen Atoms Are Key to Robust Spintronic Material
Researchers studied In2O3:Fe, a promising spintronic material, to determine what leads to its surprisingly robust magnetic properties, how to optimize it, and what to look for in other candidate spintronics materials. Read more »
On the Way to Unlimited Energy
With the help of four different ALS beamlines, scientists were able to understand and improve the morphology of the main device structure in organic photovoltaic cells. Read more »
Manganese Reduction-Oxidation Drives Plant Debris Decomposition
ALS research has shown that manganese reduction-oxidation (redox) reactions are an important factor in controlling the rate of plant debris decomposition. Understanding the role of manganese will help build better models to predict how litter decomposition rates—and thus nutrient cycling and the ecosystem carbon balance—may behave in future climate scenarios. Read more »
Porous-Framework Electrocatalysts Are Key to Carbon Dioxide Conversion
Researchers have made significant headway in the quest to convert CO2 into valuable chemical products such as fuels, pharmaceuticals, and plastics. Recent work at the ALS has shown MOFs and COFs as a valuable new class of CO2 reduction catalysts. Read more »
Spectroscopy of Supercapacitor Electrodes In Operando
X-ray spectroscopy of graphene supercapacitor electrodes under operating conditions reveals changes in electronic structure and bonding. The research could lead to an improvement in the capacity and efficiency of electrical energy storage systems needed to meet the burgeoning demands of consumer, industrial, and green technologies. Read more »
ALS X-Rays Shine a New Light on Catalysis
Recently a team of Stanford and Berkeley Lab researchers used x-rays at the ALS in a novel way to observe the behavior of electrons during technologically important chemical reactions in metal oxide electrocatalysts. What they learned has upended long-held scientific understanding of how these catalysts work. Read more »
Molecular Structure of Water at Gold Electrodes Revealed
ALS researchers have now made a first-ever observation of the molecular structure of liquid water at a gold surface under different charging conditions. This marks the first time that the scientific community has been able to achieve such high sensitivity in an in situ environment under working electrode conditions. Read more »
Infrared Mapping Helps Optimize Catalytic Reactions
A pathway to more effective and efficient synthesis of pharmaceuticals and other flow-reactor chemical products has been opened by a study in which, for the first time, the catalytic reactivity inside a microreactor was mapped in high resolution from start to finish. Read more »
Iron is the Key to Preserving Dinosaur Soft Tissue
Researchers studying organic material from dinosaur bones have been able to show that the samples contained original soft tissue material from Mesozoic dinosaurs. The x-ray techniques at the ALS were key to showing a possible mechanism for this unexpected preservation.
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