Fluoride ions show promise as charge carriers in batteries but have limited cyclability. Here we show the reversible and homogeneous topochemical insertion/deinsertion and bulk diffusion of F ions within the one-dimensional tunnels of submicrometer-sized FeSb2O4 particles at room temperature. Read more »
3D Localization of Nanoscale Battery Reactions
A new tool lets researchers pinpoint the locations of chemical reactions happening inside batteries in three dimensions at the nanoscale level. Combining ptychography, tomography, and spectroscopy, Nanosurveyor 1 is a multidimensional tool providing novel insight into the design of next-generation batteries and devices. Read more »
From Moon Rocks to Space Dust: Berkeley Lab’s Extraterrestrial Research
Berkeley Lab has a well-storied expertise in exploring samples of extraterrestrial origin. This research—which has helped us to understand the makeup and origins of objects within and beyond our solar system—stems from long-standing core capabilities in structural and chemical analyses and measurement at the microscale and nanoscale. Read more »
Ptychography of a Bacterium’s Inner Compass
Magnetotactic bacteria (MTB) synthesize chains of magnetic nanocrystals (magnetosomes) that interact with the Earth’s magnetic field like an inner compass needle, simplifying their search for optimum environments. Ptychographic spectra of magnetosomes from a marine MTB provides insight into how these inner compasses form. Read more »
Industrial-Academic Collaboration Gives Nanoscale Insight into Batteries
An industrial collaboration between Hummingbird Scientific and a team of researchers from the ALS, SLAC, Berkeley Lab, Stanford University, and other institutions has resulted in a new x-ray microscopy platform that gives scientists the ability to image nanoscale changes inside lithium-ion battery particles in real time as they charge and discharge. Insights obtained from the imaging platform have already provided surprising new insights and could help researchers improve batteries for electric vehicles as well as smart phones, laptops, and other devices. Read more »
Hewlett Packard Labs Gains Insights with Innovative ALS Research Tools
For the past eight years, Hewlett Packard Labs, the central research organization of Hewlett Packard Enterprise, has been using cutting-edge ALS techniques to advance some of their most promising technological research, including vanadium dioxide phase transitions and atomic movement during memristor operation. Read more »
X-Ray Microscopy Reveals How Crystal Mechanics Drive Battery Performance
Recent findings at the ALS show that small crystal size is key to maintaining a battery’s performance and establish soft x-ray ptychography as an essential tool for studying chemical states in nanoparticles.
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Record-Setting Microscopy Illuminates Energy Storage Materials
Using soft x-ray ptychography, researchers at the ALS have demonstrated the highest-resolution x-ray microscopy ever achieved by imaging five-nanometer structures. The researchers used ptychographic imaging to map the chemical composition of lithium iron phosphate nanocrystals, yielding important new insights into a material of high interest for electrochemical energy storage. Read more »
Concrete Industry Benefits from Ancient Romans and the ALS
New insights into the ancient Romans’ ingenious concrete harbor structures emerging from ALS beamline research could move the modern concrete industry toward its goal of a reduced carbon footprint.
Learning from Roman Seawater Concrete
Analyses of ancient concrete samples pinpointed why the best Roman concrete was superior to most modern concrete in durability, why its manufacture was less environmentally damaging, and how these improvements could be adopted in the modern world. Read more »
