We report, for the first time, sub-4 nm mapping of donor : acceptor nanoparticle composition in eco-friendly colloidal dispersions for organic electronics. This technology shows great promise for the optimization of organic semiconductor blends for organic electronics and photocatalysis and has further applications in organic core–shell nanomedicines. Read more »
ALS Work Using Microscopy/Imaging
These techniques use the light-source beam to obtain pictures with fine spatial resolution of the samples under study and are used in diverse research areas such as cell biology, lithography, infrared microscopy, radiology, and x-ray tomography.
Imaging Topological Magnetic Monopoles in 3D
Researchers created topologically stable magnetic monopoles and imaged them in 3D with unprecedented spatial resolution using a technique developed at the ALS. The work enables the study of magnetic monopole behavior for both fundamental interest and potential use in information storage and transport applications. Read more »
Macromolecular organic matter in samples of the asteroid (162173) Ryugu
We investigated the macromolecular organic matter in samples of the asteroid Ryugu—brought to Earth by the Hayabusa2 spacecraft—measuring its elemental, isotopic, and functional group compositions along with its small-scale structures and morphologies. Analytical methods used included spectro-microscopies, electron microscopy, and isotopic microscopy. Read more »
An automated size and time-resolved aerosol collector platform integrated with environmental sensors to study the vertical profile of aerosols
Researchers present the vertical distribution of size-resolved aerosol composition over an agricultural site by deploying a newly developed lightweight automated size- and time-resolved aerosol collector (STAC) platform integrated with environmental sensors on unmanned aerial systems (e.g., tethered balloon systems). Read more »
Liquid Heterostructures: Generation of Liquid–Liquid Interfaces in Free-Flowing Liquid Sheets
Microscope image of a microfluidic nozzle producing a liquid heterostructure: a layered flat liquid sheet with outer toluene layers and an inner water layer. The colored bands arise from thin film interference, indicating the presence of buried liquid‒liquid interfaces and submicron layer thicknesses. Read more »
Disorder Drives Long-Range Order in “Tetris Ice” Nanomagnet Arrays
Long-range ordering is typically associated with a decrease in disorder, or entropy. Yet, it can also be driven by increasing entropy in certain special cases. In a recent DOE-funded study, researchers demonstrated that certain artificial spin-ice arrays—nanomagnets lithographically patterned to form Tetris-like shapes—can produce such entropy-driven order. Read more »
Nanoscale Infrared Study of Meteorite Mineralogy
Using a nanoscale infrared probe, researchers found that the minerals in a meteorite—an artifact representing the solar system’s past—were altered by water on very fine spatial scales. The work sheds light on conditions in the early solar system and lays groundwork for analyzing asteroid samples to be returned to Earth by NASA in 2023. Read more »
Removing Nitrogen from Wastewater using Horizontal Levees
Treated municipal wastewater often contains nitrogen, which has been linked to algal blooms that can devastate coastal ecosystems. In a recent study, researchers characterized the primary nitrogen-removal pathways in a horizontal levee, an engineered subsurface water-treatment system consisting of a gently sloping strip of land adjacent to storm-control levees. Read more »
A Machine-Learning Approach to Better Batteries
Researchers extracted the relationship between strain and composition in a battery material by applying machine-learning methods to atomic-scale images. The work could lead to more durable batteries and also highlights the potential of integrating microscopy techniques with machine learning to gain insights into complex materials. Read more »
Key to Coral Resilience Is Faster Skeletal Crystallization
In a new study, researchers show that the crystallization rate of coral skeletons differs across species and is correlated with their resilience to ocean acidification. The results have implications for predicting coral reef survival and developing mitigation strategies against having their bony skeletons weakened by ocean acidification. Read more »
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