A variety of experiments, including ALS x-ray studies, provided direct evidence of a magnetic transition in a 2D compound called a MXene (pronounced “maxene”). The finding adds new functionality to a family of materials with numerous ways to fine-tune properties for applications ranging from spintronic devices to electromagnetic shielding. Read more »
ALS Work Using Microscopy/Imaging
These techniques use the light-source beam to obtain pictures with fine spatial resolution of the samples under study and are used in diverse research areas such as cell biology, lithography, infrared microscopy, radiology, and x-ray tomography.
Xylella fastidiosa causes transcriptional shifts that precede tylose formation and starch depletion in xylem
During Pierce’s disease, Xylella fastidiosa triggers transcriptional changes in grapevines and induces major physiological responses, including tylose formation and starch depletion. X-ray computed microtomography and a machine-learning algorithm were used to track the depletion of starch reserves in the xylem of a grapevine stem infected with Pierce’s disease. Read more »
Unique X-Ray Microscope Reveals Dazzling 3D Cell Images
Researchers used soft x-ray tomography to reveal never-before-seen details about insulin secretion in pancreatic cells taken from rats. By quantifying subcellular rearrangements in response to drugs, the results are an important first step for bridging the longstanding gap between structural biology and physiology. Read more »
Coordinated decline of leaf hydraulic and stomatal conductances under drought is not linked to leaf xylem embolism for different grapevine cultivars
Drought decreases water transport capacity of leaves and limits gas exchange, which involves reduced leaf hydraulic conductance (Kleaf) in both the xylem and outside-xylem pathways. We combined Kleaf and gas exchange measurements, micro-computed tomography of intact leaves, and spatially explicit modeling of the outside-xylem pathways to evaluate the role of vein embolism and Kleaf in the responses of two different grapevine cultivars to drought. Read more »
From Stripes to Skyrmions in a Surprising Material
Researchers showed that tiny bubbles of ordered spins (skyrmions) can be induced to form in a material previously considered incompatible with skyrmion formation. The discovery opens up a new class of material systems that exhibit technologically desirable nanoscale features attractive for spintronic applications. Read more »
Super-Resolution Measurement of X-Ray Mirrors
ALS researchers, in collaboration with software and nanofabrication small businesses, developed a way to improve the accuracy of instruments that measure the surfaces of x-ray mirrors. The work significantly improves the quality of the data needed for the fabrication and optimal performance of advanced x-ray beamlines and space telescopes. Read more »
Microstructures Explain Beetle Exoskeleton Strength
Using microtomography and other techniques, researchers identified the exoskeletal toughening mechanisms that explain the crush resistance of the aptly named diabolical ironclad beetle. The observations could be applied in developing tough, impact- and crush-resistant materials for joining dissimilar materials. Read more »
Evidence of a magnetic transition in atomically thin Cr2TiC2Tx MXene
2D magnetic materials have recently attracted significant interest as model systems to understand low-dimensional magnetism and for potential spintronic applications. Here, we report on synthesis of Cr2TiC2Tx MXene and a detailed study of its magnetic as well as electronic properties. Read more »
X-Rays Reveal Architectural Clues to the Crush-Resistance of Diabolical Ironclad Beetles
The appropriately named diabolical ironclad beetle has an incredibly crush-resistant exoskeleton, which could serve as a blueprint for tougher materials. To see, in microscopic detail, what makes the beetle so uniquely ironclad, researchers used the ALS to explore a protective covering known as the “elytra,” its abdomen, and other parts. Read more »
Design and synthesis of high performance flexible and green supercapacitors made of manganese‐dioxide‐decorated alkali lignin
Researchers synthesized a plant‐based composite electrode for use in flexible supercapacitors and used synchrotron x‐ray microtomography to better understand the impact of microstructure and morphology on electrode porosity and electrical conductance. Read more »
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