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ALS Work Using Spectroscopy

These techniques are used to study the energies of particles that are emitted or absorbed by samples that are exposed to the light-source beam and are commonly used to determine the characteristics of chemical bonding and electron motion.

 

Molecular Framework Imparts Stability to Reactive Catalyst

Researchers have shown that a rigid metal–organic framework (MOF) can be used to stabilize core regions of a reactive catalyst that has potential for use in artificial photosynthesis. The framework immobilizes and preserves key reactive intermediates and affords a clearer view of how the catalyst’s structure correlates with function. Read more »

Catalyst Improves Cycling Life of Magnesium/Sulfur Batteries

Magnesium/sulfur batteries hold promise as a safer, energy-dense advancement, but previous iterations have suffered from extremely limited recharging capabilities. Studies at the ALS provided electrochemical insights into battery polarization and revealed how a titanium catalyst activates magnesium/sulfur compounds to improve battery performance. Read more »

Here Comes the Sun: A New Framework for Artificial Photosynthesis

Scientists have long sought to mimic the process by which plants make their own fuel using sunlight, carbon dioxide, and water through artificial photosynthesis devices, but exactly how catalysts work to generate renewable fuel remains a mystery. Now, a study has uncovered new insight into how to better control cobalt oxide, one of the most promising catalysts for artificial photosynthesis. Read more »

Clues to the Early Solar System Preserved in a Meteorite

Scientists analyzing a tiny carbon-rich pocket inside a meteorite found unexpected chemical signatures. Their findings are the first direct evidence that material from the outer solar system may have traveled inward long before planets formed, providing insight into the early solar system. Read more »

A New Path to Carbon Dioxide Transformation

Combining ALS experiments with quantum-mechanical calculations, scientists found dramatic differences in how carbon dioxide (CO2) reactions begin on silver as opposed to copper. Both metals help transform CO2—a greenhouse gas—into more useful forms, and this new atomic-level data could help make the process more efficient. Read more »PPT-icon-35 PDF-icon-35

Chiral Crystals Give Rise to Topological Conductors

Researchers have discovered materials whose chiral crystal structures produce chirality in their electronic behavior. These topological conductors retain their unique electronic properties regardless of defects and open new possibilities in materials research. Read more »

Infrared Light Reveals Microstripes at Insulator-Metal Transition

In this study of a current-driven insulator-to-metal transition, a distinctive stripe pattern develops between the insulating and metallic phases. The work reveals remarkable new features of electrically induced insulator-to-metal transitions in materials with potential applications in energy-efficient memory and transistor devices. Read more »PPT-icon-35

Evidence of a Long-Predicted Magnet

Half a century ago, theorists proposed a novel way for materials to produce a magnetic field. Now, scientists have discovered a uranium compound that bears out that long-ago theory—a new type of magnet that holds promise for enhancing the performance of data storage technologies. Read more »

The Best Topological Conductor Yet: Spiraling Crystal Is the Key to Exotic Discovery

Researchers have discovered the strongest topological conductor yet, in the form of thin crystal samples that have a spiral-staircase structure. The realization of so-called topological materials—which exhibit exotic, defect-resistant properties and are expected to have applications in electronics, optics, quantum computing, and other fields—has opened up a new realm in materials discovery. Read more »

Fingerprint Oxygen Redox Reactions in Batteries through High-Efficiency Mapping of Resonant Inelastic X-ray Scattering

We provide a comprehensive analysis and an explicit interpretation of the five evolving components of O-K mRIXS of the typical battery electrode that involves lattice oxygen redox reactions upon cycling. This work is the first benchmark for a complete assignment of all the important mRIXS features collected from battery materials, and thus delivers guidelines for future studies of oxygen redox reactions. Read more »