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ALS Work Using Scattering/Diffraction

These techniques make use of the patterns of light produced when x-rays are deflected by the closely spaced lattice of atoms in solids and are commonly used to determine the structures of crystals and large molecules such as proteins.

 

Surtsey Volcano: A Rare Window into Earth’s Oceanic Crust

Surtsey, a very young oceanic island in Iceland, emerged through explosive volcanic activity in 1963. Utilizing various techniques, including x-ray microdiffraction at the ALS, researchers gained unique insights into the transformation of volcanic glass to form mineral cements in the basaltic rock of underwater volcanoes. Read more »

New Insights Lead to Better Next-Gen Solar Cells

Perovskites show great promise to reduce the costs of solar power but are not yet durable enough to be commercially viable. Researchers used simultaneous characterization techniques to understand why a simplified fabrication process works so well, providing key insights to nudge perovskites closer to commercialization. Read more »

Bifurcation of High- and Low-Energy Electrons in Microbial Metabolism

A class of chemical reaction found only in biology, electron bifurcation channels two electrons from one donor to two separate acceptors, with one electron elevated in energy at the expense of lowering the energy of the second. Researchers used the ALS to study this process in a microbial protein involved in this bioenergetic pathway. Read more »

The Effects of Diabetes on Spinal-Column Biomechanics

Researchers found that type 2 diabetes induces earlier onset of plastic (nonrecoverable) deformation in intervertebral discs by impairing the biomechanical behavior of collagen. A greater understanding of the underlying causes of tissue failure in diabetes—a growing problem worldwide—is important in helping to prevent and treat symptoms. Read more »PPT-icon-35

How Processing Affects Structure in Composite Nanotube Yarns

Using the ALS, researchers found quantitative correlations between processing parameters and the structure of ultrafine, polymer-reinforced carbon-nanotube fibers. The work will facilitate the production of high-strength materials, including those needed for positioning target capsules for fusion research at the National Ignition Facility. Read more »PPT-icon-35 PDF-icon-35

A Bio-Inspired Metal-Organic Framework for Capturing Wellhead Gases

Burning of natural gas at oil and gas wells, called flaring, is a major waste of fossil fuels and a contributor to climate change. In this work, researchers synthesized and characterized a metal-organic framework that uses biomimetic chemistry to convert wellhead gases into economically valuable feedstocks for petrochemical products. Read more »

Tracking Platinum Movement on Fuel-Cell Electrodes

Researchers tracked the movement of the platinum nanoparticles that catalyze reactions in polymer electrolyte fuel cells (PEFCs) and correlated this movement with nanoparticle degradation. The results yielded solutions that can immediately reduce platinum waste in emission-free heavy-duty fuel-cell vehicles. Read more »PPT-icon-35 PDF-icon-35

Computer-Aided Protein Design for New Biomaterials

Using a computer-based approach, researchers designed porous protein crystals that were revealed to be stable, tunable, and atomically accurate using x-ray scattering and diffraction at the ALS. The work provides a powerful new platform for biological materials engineering and opens up wide applications in biotechnology and medicine. Read more »PPT-icon-35 PDF-icon-35

Immune Response Spurs Growth of “Soft” Kidney Stones

Matrix stones are an unusual type of soft kidney stone closely associated with the presence of bacteria from unchecked urinary tract infections. Researchers conducted a comprehensive study of surgically extracted matrix stones, work that highlights how host defense mechanisms against microbes can simultaneously encourage harmful stone formation. Read more »