A new, in-beamline spin-coating platform enabled researchers to probe the structure of a promising photovoltaic material in the crucial early stages of processing. The results demonstrate the power of multimodal in situ techniques as promising tools for optimizing synthesis parameters and, thus, device performance. Read more »
Freeze Frame: Scientists Capture Atomic-Scale Snapshots of Artificial Proteins
Protein-like molecules called polypeptoids have great promise as precision building blocks for creating a variety of designer nanomaterials. In this study, rsearchers used cryo-EM, a technique originally designed to image proteins in solution, as well as x-ray scattering techniques, to characterize the structure of polypeptide nanosheets. Read more »
Nobumichi Tamura Receives 2019 Klaus Halbach Award
Nobumichi Tamura received the 2019 Klaus Halbach Award in recognition for the software he developed to analyze microdiffraction data. The first version of the software was completed just before Christmas 1999 and has been a gift for many in the community ever since. Read more »
Newly Discovered Minerals Reveal Anomalous Origins
Researchers characterized two highly unusual nickel-containing minerals, both unearthed in an ancient geological site in southern central Siberia. The findings extend our understanding of naturally occurring mineral species and varieties and provide useful insights into the environments leading to the formation of potentially valuable mineral ores. Read more »
Mineral Discovery Made Easier: X-Ray Technique Shines a New Light on Tiny, Rare Crystals
Like a tiny needle in a sprawling hayfield, a single crystal grain measuring just tens of millionths of a meter— found in a borehole sample drilled in Central Siberia—had an unexpected chemical makeup. And a specialized x-ray technique in use at the ALS confirmed the sample’s uniqueness and paved the way for its formal recognition as a newly discovered mineral: ognitite. Read more »
Study Concludes Glassy Menagerie of Particles in Beach Sands Near Hiroshima is Fallout Debris from A-Bomb Blast
Mario Wannier was methodically sorting through particles in samples of beach sand from Japan’s Motoujina Peninsula when he spotted something unexpected: a number of tiny, glassy spheres and other unusual objects. X-ray studies have provided evidence that they are A-bomb fallout from the destroyed city of Hiroshima. Read more »
Imaging Magnetic Microstructure Response to Substrate Strain
A ferromagnetic thin film on a piezoelectric substrate offers a way to control magnetization in ultralow-power devices by relying on coupling between the piezoelectric and ferromagnetic components. At the ALS, researchers were able to image the electrically induced magnetic behavior and correlate it with the piezo-strain driving it. Read more »
The Microstructure of a Parrotfish Tooth Contributes to Its Toughness
Parrotfish chew on coral, producing hundreds of pounds of sand each year. Mapping the microstructure of parrotfish teeth, scientists found bundles of crystals interwoven like chain mail. The results provide a blueprint for creating ultra-durable materials for mechanical components that undergo repetitive contact, movement, and abrasion. Read more »
Coral Exoskeleton Growth Begins Inside Living Tissue
Researchers have discovered some good news regarding corals: the mechanism by which their exoskeletons grow may help them resist the effects of ocean acidification. The discovery, made with PEEM studies, has ramifications not only for the health of coral reefs, but for applications such as 3D printing as well. Read more »
X-Rays Reveal the Biting Truth About Parrotfish Teeth
A parrotfish’s hardy teeth allow it to chomp on coral all day long, ultimately grinding it up through digestion into fine sand. Researchers wanting to see how the fine crystal structure of parrotfish teeth contribute to their incredible strength were able to visualize the orientation of individual crystals, which showed their intricately woven structure. Read more »
